Synthesis, Characterization of Some New 1-Phenyl (3-Chloro- 4-Methoxy, 2-Methoxy-5-Methyl)- 4(Substituted) Phenyl Benzene-Azo Acetyl Acetone-3,5-Dimethyl Pyrazoles


Alok K. Pareek*, P. E. Joseph and Daya S. Seth
School of Chemical Sciences, Department of Chemistry, ST. John’s College, Agra - 282 002 India.

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ABSTRACT:

This review introduces the synthesis of some newly 1-phenyl (3-chloro-4-methoxy, 2-methoxy-5-methyl)- 4(substituted) phenyl benzeneazo acetyl acetone-3,5-dimethyl pyrazoles (4a-4l, 5a-5l) containing different selected functional groups have been synthesized by condensing (3-chloro-4-methoxy, 2-methoxy-5-methyl) phenyl benzeneazo acetyl acetone hydrazone (1a,2a) with (RI) -malon phenyl anilic acid hydrazide (3a-3i,3j,3j1,3k,3k1-3l) in alcoholic medium, presence of glacial acetic acid as a catalyst. The identity of newly synthesized compounds were confirmed on the basis of their spectral studies viz- IR, physical properties, elemental analysis.

KEYWORDS:

Synthesis; Substituted Acetyl Acetone Hydrazones; Substituted Acid Hydrazides; Characterization; GAA, Condensation; Pyrazoles; Spectral Analysis


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