Spectrophotometric determination of Fe(II) as a complex with 1, 2 -propanedione, 1-phenyl -1-( 2-hydroxybenzylideneazine ) – 2 – oxime (PDPHBAO)

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Spectrophotometric determination of Fe(II) as a complex with 1, 2 -propanedione, 1-phenyl -1-( 2-hydroxybenzylideneazine ) – 2 – oxime (PDPHBAO)

Rama S. Lokhande, Sushama M. Lele and Poonam P. Shevde

Department of Chemistry, University of Mumbai, Vidyanagri, Santacruz (E), Mumbai - 400 098 (India).

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ABSTRACT:

The reagent was synthesized and characterization was carried out by FTIR, NMR, elemental analysis as well as Mass spectrometry. This reagent was then applied for the development of the analytical method for the extractive spectrophotometric determination of Iron (II). Iron metal forms faint yellowish green coloured complex, which can be extracted in chloroform at pH 10.0 having absorption maxima at 536 nm. Beer

KEYWORDS:

Characterization; Iron; Extractive spectrophotomertic determination