Synthesis, Ion Exchange Properties and Analytical Application of New Hybrid Cation Exchanger : Acrylonitrile Tin(IV)Tungstophosphate

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Synthesis, Ion Exchange Properties and Analytical Application of New Hybrid Cation Exchanger : Acrylonitrile Tin(IV)Tungstophosphate

Md. Mahboob Ahmad, Weqar Ahmad Siddiqui and T. A. Khan

Department of Applied Sciences and Humanities, Faculty of Engineering and Technology, Jamia Millia Islamia, New Delhi -110 025 (India).

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ABSTRACT:

A new hybrid inorganic-organic cation exchanger acrylonitrile tin (iv) tungstophosphate has been synthesized and its analytical application explored. The effect of experimental parameter such as reagent mixing ratio, temperature effect on ion exchange properties of material has been studied. The material behaves as monofunctional acid with ion exchange capacity of 1.91 and 1.94 meq g-1 was found to be for Na+ and K+ respectively. The chemical stability data reveals that the exchanger is quite stable in mineral acid, bases and fairly stable in organic solvent, whereas thermal analysis shows that the material retain 78.65 % I.E.C upto 400

KEYWORDS:

hybrid ion exchanger ; acrylonitrile tin (iv) tungstophosphate; Pb+2 and Sr+2 selective