Abstract
Synthesis and Characterization of Polyesteramide urethane derived from Melia Azedarach seed oil
Sageer Ahamad, Ghazala Imran, S. A. Ahmad and A. Hasnat*
DOI : http://dx.doi.org/10.13005/ojc/310271
Abstract:
Polyesteramide urethane resin has been synthesized from a nontraditional Malia Azedarach seed oil. The oil converted to N,N-bis (2-hydroxy ethyl) maleia azedrach oil fatty acid (HEMFA) by reacting with diethanol amine. HEMFA reacted with phthalic acid to obtained Malia Azedarach polyesteramide (MAPEA). The MAPEA treated with toluene-2,4-diisocyanate (TDI) in different ratios to synthesized polyesteramide urethane (MAPEAU). The optimum wt-% ratio of the TDI to the MAPEA is selected on the basis fluidity and film properties of the MAPEAU. The synthesized intermediates and final resin have been characterized by FT-IR, 1HNMR spectroscopic analyses and by the measurement of physic-chemical properties like specific gravity, refractive index, acid value, iodine value, soponification value.
Keywords:Malia Azedarach; Vegetable oil; Polyesteramide; Urethane
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