Abstract

Manisha R. Sawant^1*, Suresh T. Gaikwad²,Sushama B. Dare¹and Anjali S. Rajbhoj²

DOI : http://dx.doi.org/10.13005/ojc/360213

The present work aims to synthesize 2,5–disubstituted-1,3,4–oxadiazoles using electrochemically prepared nanoparticles of nickel oxide as catalyst. The nanoparticles thus prepared using electrochemical syntheses are in appreciable yield. The tetrabutyl phosphonium bromide has been used for capping followed by UV, FTIR, XRD, SEM EDS and TEM SAED studies for the characterization. The 2,5-disubstituted-1,3,4-oxadiazoles were synthesized from substituted benzoic acids and their hydrazides in microwave synthesis system using prepared nanoparticles as a catalyst.

Electrochemical Synthesis; 2, 5–Disubstituted-1, 3, 4-Oxadiazoles; Nickel Oxide Nanoparticles; Tetrabutyl Phosphonium Bromide

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