ISSN : 0970 - 020X, ONLINE ISSN : 2231-5039
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Abstract

X-ray Diffraction Studies of Co(II), Sm(III) and Nd(III) Complexes with Gliclazide (N-(hexahydrocyclopenta[c] pyrrol-2(1H)-carbamoyl)-4-methylbenzenesulfonamide, An Oral Antidiabetic Drug

Bal Krishan1*, M. Tawkir1 and S.A. Iqbal2


Abstract:

Gliclazide(N-hexahydrocyclopentapyrrol-2-carbamoyl)-4-methylbenzenesulphonamide was used to synthesize Co(II),Sm(III) , Nd(III) complexes. Metal complxes were characterized by elemental analysis, IR, NMR,TGA. The crystal structure of complexes were further determined by X-ray diffraction method. The XRD data was used to calculate various parameters like crystal system, volume,density,porosity,particle size etc.which shows that the complexes of Co(II),Sm(III) and Nd(III) are octahedral structure.

Keywords:

Gliclazide; Crystal structure; Co(II); Sm(III) and Nd(III) complex

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