ISSN : 0970 - 020X, ONLINE ISSN : 2231-5039
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Abstract

Effect of Drying on the Synthesis and Characterization of MoVTeNbOx Mixed Metal Oxide Catalysts Prepared by Reflux

Irmawati Ramli1,2*, Che Ku Nor Liana Che Ku Hitam1 , Hossein Abbastabar Ahangar1,3 and Abdul Halim Abdullah2


Abstract:

MoVTeNb mixed oxide catalysts were successfully prepared by reflux with different drying methods. X-ray diffraction (XRD) confirmed the presence of orthorhombic (M1), hexagonal (M2) and (Mo0.93V0.07) 5 O14 phases after spray drying the slurry, while the catalysts obtained from the precipitate and mother liquid contained only hexagonal M2 and (Mo0.93V0.07) 5 O14 phases. Temperatureprogrammed reaction (TPRn) analysis and catalytic test identified the highest activity in the sample synthesized by spray drying in the partial oxidation of propane to acrylic acid.

Keywords:

MoVTeNb mixed metal oxide; reflux; propane oxidation

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